|
The LSP operates the following main
equipment (as of 31 May 2007)
|
High Throughput Olefin Polymerization Catalyst
Screening
|
 |
·
Symyx PPR24® Polyolefin Workflow*
* 24 individually controlled parallel olefin
polymerization microreactors (40 bar, 200°C) with
dual injector ports (for solutions and slurries)
Triple glove-box configuration for doubling to PPR48
configuration
Dual arm integrated liquid handling robot (with
solution and slurry injection needles)
Integrated Bohdan Robotic Weighing Station
Off-line Integrated HT-GPC and NMR Tools
Genevac EZ-2 Polymer Drying Station
MBraun SPS-5 Solvent Purification System
Symyx Software (PPR Client®, Library
Studio®, PolyView®, Epoch®,
Impressionist®, Symyx Renaissance
Application Server)
Oracle Database Server
|
Olefin Polymerization Reactors
|
 |
·
Computer-Monitored 2 L Stainless Steel Batch
Reactor (Brignole Mod.
AU-2 ; 200 bar, 300°C)
·
Computer-Monitored 1 L Stainless Steel Batch
Reactor (Brignole Mod.
AU-1 ; 200 bar, 300°C)
·
0.30 L Stainless Steel Batch Reactor (Brignole Mod.
AU-0.30 ; 100 bar, 200°C)
·
0.15 L Stainless Steel Batch Reactor (Brignole Mod.
AU-0.15 ; 100 bar, 200°C)
Controlled Atmosphere Equipment
·
Braun Lab-Master Glove-Boxes
·
Vacuum-Atmospheres Glove-Box
NMR Spectroscopy
·
600 (3)*, 500, 400, 300, 200 (3)** MHz
Spectrometers (Shared Access)
* 1 with HT 8 mm probe, 1 with HR-MAS and CP-MAS
probe, 1 with Cryo-Probe
** 1 dedicated to CP-MAS
·
400 MHz (Bruker Avance DRX 400) Spectrometer (LPS-Owned)
·
Proprietary Software for Spectral Simulation
(SHAPE2000 Package) and for Statistical Analysis of
Polyolefin Microstructure (ConfStat and CopolStat
packages)
X-Ray Diffraction
·
Single-Crystal Diffractometers (2)* (Shared
Access)
* 1 with Area Detector
·
Automatic Powder Diffractometers (2)** (Shared
Access)
** 1 with VT Cell, 1 with Controlled-Atmosphere
Cell
Thermal Analysis
·
DSC (2)*, DSC/TGA**, DMTA*** (Shared access)
* Perkin Elmer Pyris 1, Perkin-Elmer DSC-7
** Mettler DSC822/DSC30/TG50, with Low-Temperature
DSC Cell
*** Polymer Lab
Gel Permeation Chromatography
·
Waters Alliance GPCV2000 Chromatograph with dual
detection system
Mass Spectrometry
·
Access to the Inter-Department Large Scale
European MS Facility (“All” Tools)
Computing Facilities
·
Clusters of Opteron units (80 CPUs)
·
HP ES45 Parallel Computers (48 CPUs; Shared
Access) |